Difference between revisions of "Walk-up NMR user instructions for Bruker"

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# when the list of solvents appears, choose the one that your sample is in
 
# when the list of solvents appears, choose the one that your sample is in
 
# once the sample is locked, type topshim on the command line to shim the sample
 
# once the sample is locked, type topshim on the command line to shim the sample
# while the sample is being automatically shimmed,
+
# while the sample is being automatically shimmed, type edc on the console to create a new file
 +
# edc opens the window that sets everything for the experiment to run your sample

Revision as of 00:14, 13 May 2020

Introduction

If you need to use a Bruker NMR instrument for a liquid sample, here are some quick instructions to get your sample running as easily as possible:

  1. log in to workstation
  2. log in to TopSpin
  3. type ej on the command line or click the eject button to eject the current sample that is in the magnet
  4. remove the old sample from the top of the magnet
  5. remove the old sample from the sample holder
  6. place your sample in the sample holder
  7. slide your sample down in the holder until it hits the stop
  8. place the sample/holder on top of the column of air on the magnet
  9. go back to the workstation, click insert sample and wait for the sample to drop down into the probe
  10. type lock on the command line
  11. when the list of solvents appears, choose the one that your sample is in
  12. once the sample is locked, type topshim on the command line to shim the sample
  13. while the sample is being automatically shimmed, type edc on the console to create a new file
  14. edc opens the window that sets everything for the experiment to run your sample