Difference between revisions of "Walk-up NMR user instructions for Bruker"
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# when the list of solvents appears, choose the one that your sample is in | # when the list of solvents appears, choose the one that your sample is in | ||
# once the sample is locked, type topshim on the command line to shim the sample | # once the sample is locked, type topshim on the command line to shim the sample | ||
− | # while the sample is being automatically shimmed, | + | # while the sample is being automatically shimmed, type edc on the console to create a new file |
+ | # edc opens the window that sets everything for the experiment to run your sample |
Revision as of 00:14, 13 May 2020
Introduction
If you need to use a Bruker NMR instrument for a liquid sample, here are some quick instructions to get your sample running as easily as possible:
- log in to workstation
- log in to TopSpin
- type ej on the command line or click the eject button to eject the current sample that is in the magnet
- remove the old sample from the top of the magnet
- remove the old sample from the sample holder
- place your sample in the sample holder
- slide your sample down in the holder until it hits the stop
- place the sample/holder on top of the column of air on the magnet
- go back to the workstation, click insert sample and wait for the sample to drop down into the probe
- type lock on the command line
- when the list of solvents appears, choose the one that your sample is in
- once the sample is locked, type topshim on the command line to shim the sample
- while the sample is being automatically shimmed, type edc on the console to create a new file
- edc opens the window that sets everything for the experiment to run your sample