Difference between revisions of "Walk-up NMR user instructions for ThermoFisher"
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| − | The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample: | + | The [[NMR Instrument Manufacturers|picospin]] tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample: |
# Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present. | # Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present. | ||
# Check to make sure a filter is properly connected and a collection flask is at the "out" port. | # Check to make sure a filter is properly connected and a collection flask is at the "out" port. | ||
# Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port. | # Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port. | ||
# Go to the picospin page of the web browser interface | # Go to the picospin page of the web browser interface | ||
| − | # Select the '''Files'''option. | + | # Select the '''Files''' option. |
# Select the '''Standard Run''' option. | # Select the '''Standard Run''' option. | ||
# Click '''Use these settings at run'''. | # Click '''Use these settings at run'''. | ||
Latest revision as of 03:37, 25 May 2020
The picospin tabletop NMR instruments utilize an injection system for samples rather than the usual 5mm NMR tubes. The instrument also has a web-based interface for control and processing. Here are some instructions to get a quick spectrum of your sample:
- Fill a 1mL plastic syringe approximately half way. Be sure to remove any air bubbles that may be present.
- Check to make sure a filter is properly connected and a collection flask is at the "out" port.
- Slowly inject your sample into the "in" port until you observe a few drops coming out of the "out" port.
- Go to the picospin page of the web browser interface
- Select the Files option.
- Select the Standard Run option.
- Click Use these settings at run.
- The Run page will appear.
- Check the transmitter frequency and set the scans.
- Click Start Run.
- Process spectra with MNova, which is included with the product.
